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Chlorobenzene by NIOSH 1003M

Category Industrial Hygiene (IH) Lab Services
Test Chlorobenzene by NIOSH 1003M

Issue 3: 15 March 2003

  • This method utilizes a charcoal tube (226-01) for collection of vapors, desorption with carbon disulfide and analysis by gas chromatography with flame ionization detection. 
  • NIOSH recommends 2-10 field blanks be submitted to the laboratory with each sampling event. 
  • Samples do not need to be refrigerated but should be packed properly to ensure no breakage occurs. 
  • Samples must be labeled individually. 
  • NIOSH indicates that the samples must be analyzed within 30 days of sampling.

If you need more information this method can also be found at:

CAS Number 628-63-7
Test Type Single
Test Prefix n-
Test Amyl Acetate
Synonym(s) Amyl Acetate; Pentyl Acetate
Method EMSL In-House Method; SOP VOCs by GC
Matrices Tubes
Group Package
Cinnaminson New Jersey - Corporate Lab (IH LAB 28)
Huntington Beach California (LAB 33) X
Indianapolis Indiana (LAB 16) X
Charlotte (Pineville) North Carolina (LAB 41)
Minneapolis (New Hope) Minnesota (LAB 10) 101103
Toronto Ontario Canada (LAB 55)
Chromotography Type / Detector GC-FID
OSHA PEL or Other Value in mg/m3 266
OSHA PEL or Other Value in µg/m3 266000
OSHA PEL or Other Value in ppm 49.96
OSHA or Most Relevant OEL Notes 50 ppm ACGIH TLV TWA 100 ppm ACGIH STEL
Sampling Instructions / Interferences Protect from heat, ship cold (5C).
Method link
Molecular Weight - grams/mol 130.19
Reporting Limits (Field Blank Limit) ug/sample 3
LOQ (ug/sample based on media)/sample 2
Default Reporting Units ppm

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