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Soot Testing, Wildfire Smoke Testing, Smoke Damage

Category Materials Testing Lab
Test Soot
Description

In recent years, there has been an increasing number of complaints relating to the sudden and unexpected appearance of soot-like material observed in homes and commercial buildings.  These stains may form on carpets, walls, plastic objects and other materials, and have been noted around ventilation grilles and electrical outlets.  The culprit for this “ghosting” phenomenon is the formation of Black Carbon.   EMSL Analytical, Inc. has extensive experience in confirming the presence and identifying the source of Black Carbon.

 

Black Carbon is a fine-grained solid residue that results from incomplete combustion of hydrocarbons.  Common sources of Black Carbon that can cause residential or commercial property damage include candles, fuels such as oil, propane and natural gas used in gas appliances and gas log fireplaces, firewood burned in a fireplace or a wood-burning stove.  Even printer cartridges can produce a manufactured Carbon Black that is nearly identical to Black Carbon (Soot).

 

Black Carbon particles may appear as individual spherical particles or as grape-like conglomerates.   The diameter of the individual particles generally varies between 10nm to 70nm.  Considering the size and the specific morphology of Black Carbon particulate, the analysis for identification of Black Carbon is best performed by electron microscopy ensuring the appropriate magnification range for imaging.  Transmission Electron Microscopy can easily achieve a magnification of 100,000x, which is more than sufficient to observe individual particles.  Even the best light microscopes can only achieve 1,000x magnification.  At a magnification of 1000x observations are limited to particles no smaller than 300nm.  This is roughly the size of the smallest bacteria.  Black Carbon particles are generally one order of magnitude smaller.

 

However, the majority of nano-size particles, such as iron oxides, titanium dioxide or aluminum oxide have the same morphology.  For example, titanium dioxide (TiO2) is a common interference due to its spherical morphology and its expansive use in food, commercial and pharmaceutical products.  Therefore, the particles elemental composition should also be determined by energy dispersive x-ray analysis to verify if the material sampled is actually Black Carbon.

 

At EMSL Analytical, Inc. identification of Black Carbon is performed using Transmission Electron Microscopy (TEM) in conjunction with Energy Dispersive X-Ray Analysis (EDX).  Sample collection for airborne Black Carbon should be performed according to the NIOSH 5000 method.  Dust “wipe” sampling can be performed with 1 square inch alcohol wipes such as those used to cleanse your arm before a shot with a hypodermic needle. These can be found at nearly any pharmacy.
 

Identifying the origin of combustion product formation can help to eliminate potential sources.  At EMSL Analytical, Inc., the identification of the source of Black Carbon is performed using Transmission Electron Microscopy (TEM) in conjunction with Attenuated Total Reflection - Fourier Transform Infrared Spectroscopy (ATR-FTIR) and Gas Chromatography / Mass Spectrometry (GC/MS).  The analysis is based upon the different particle sizes and the presence of selected functional groups in the samples that distinguish sources such as paraffin residue from candles or fuel oil from oil heaters.

 

Laboratories performing Soot / Carbon Black Analysis

Cinnaminson, NJ

San Leandro, CA

South Pasadena, CA


Ann Arbor, MI (LAB 08) - NVLAP Lab Code 101048-4Atlanta, GA (LAB 07) - NVLAP Lab Code 101048-1Baton Rouge, LA (LAB 25) - NVLAP Lab Code 200375-0Beltsville, MD (LAB 19) - NVLAP Lab Code 200293-0Boston, MA (LAB 13) - NVLAP Lab Code 101147-0Buffalo, NY (LAB 14) - NVLAP Lab Code 200056-0Carle Place, NY (LAB 06) - NVLAP Lab Code 101048-10Charlotte, NC (LAB 41) - NVLAP Lab Code 200841-0Chicago, IL (LAB 26) - NVLAP Lab Code 200399-0Cinnaminson, NJ (LAB List in Description) - NVLAP Lab Code 101048-0Dallas, TX (LAB 11) - NVLAP Lab Code 600111-0Denver, CO (LAB 22) - NVLAP Lab Code 200828-0EMSL Canada - Calgary, AB (LAB 65) - NVLAP Lab Code 500100-0EMSL Canada - Montreal, QC (LAB 68) - NVLAP Lab Code 201052-0EMSL Canada - Ottawa, ON (LAB 67) - NVLAP Lab Code 201040-0EMSL Canada - Toronto, ON (LAB 55) - NVLAP Lab Code 200877-0EMSL Canada - Vancouver, BC (LAB 69) - NVLAP Lab Code 201068-0Fort Lauderdale, FL (LAB 56) - NVLAP Lab Code 500085-0Houston, TX (LAB 15) - NVLAP Lab Code 102106-0Huntington Beach, CA (LAB 33) - NVLAP Lab Code 101384-0Indianapolis, IN (LAB 16) - NVLAP Lab Code 200188-0Inland Empire, CA (LAB 71) - NVLAP Lab Code 600239-0Jacksonville, FL (LAB 54) - NVLAP Lab Code 600265-0Kernersville, NC (LAB 02) - NVLAP Lab Code 102104-0Las Vegas, NV (LAB 31) - NVLAP Lab Code 600140-0Miami, FL (LAB 17) - NVLAP Lab Code 200204-0Minneapolis, MN (LAB 35) - NVLAP Lab Code 200019-0New York, NY (LAB 03) - NVLAP Lab Code 101048-9Orlando, FL (LAB 34) - NVLAP Lab Code 101151-0Phoenix, AZ (LAB 12) - NVLAP Lab Code 200811-0Piscataway, NJ (LAB 05) - NVLAP Lab Code 101048-2Plymouth Meeting, PA (LAB 18) - NVLAP Lab Code 200699-0Raleigh, NC (LAB 29) - NVLAP Lab Code 200671-0Rochester, NY (LAB 53) - NVLAP Lab Code 600183-0Salem, NH (LAB 23) - NVLAP Lab Code 201051-0San Diego, CA (LAB 43) - NVLAP Lab Code 200855-0San Leandro, CA (LAB 09) - NVLAP Lab Code 101048-3Seattle, WA (LAB 51) - NVLAP Lab Code 200613-0South Pasadena, CA (LAB 32) - NVLAP Lab Code 200232-0South Portland, ME (LAB 62) - NVLAP Lab Code 500094-0St. Louis, MO (LAB 39) - NVLAP Lab Code 200742-0Tampa, FL (LAB 93) - NVLAP Lab Code 600215-0Wallingford, CT (LAB 24) - NVLAP Lab Code 200700-0West Palm Beach, FL (LAB 57) - NVLAP Lab Code 600206-0Weymouth, MA (LAB 64) - NVLAP Lab Code 600217-0
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